反应详情

To a mixed solution of methyl 3-ethoxy-4-nitrobenzoate (6.05 g) in methanol (100 ml) and THF (100 ml) was added 10% Pd/C (50% wet, 0.60 g), and the mixture was stirred under a hydrogen atmosphere overnight. The reaction mixture was filtered through celite, and the filtrate was evaporated under reduced pressure to give a crude product (5.21 g) of the title compound. The obtained crude product was used for the next reaction without further purification.

1. filtrationThe reaction mixture was filtered through celite
2. customthe filtrate was evaporated under reduced pressure
3. customto give a crude product (5.21 g) of the title compound
4. customThe obtained crude product
5. customwas used for the next reaction without further purification