HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-benzyloxycarbonylamino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one → 3-Amino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-benzyloxycarbonylamino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one | HCID 13375105 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 3-Amino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one | HCID 357334 | — |
Reaction Steps
1.0 g of 3-benzyloxycarbonylamino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one was dissolved in 20 ml of methanol and then hydrogenated at atmospheric pressure in the presence of 50 mg of 5% palladium-carbon. Thus, there was obtained the desired compound, or 3-amino-2,3-dihydro-1,5-benzothiazepin-4(5H)-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539151 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-ca91a323ecab4a5f8a1d788457d863e8 |
| Source note | uspto-grants-1985_09 |