Water → HCID 10947700, compound

Participants

Reaction Conditions

Reaction Steps

39 g (0.5 mole) of sodium sulfide were added to 47.8 g (0.1 mole) of the tosylate of 1,1-bis-(4-chlorophenoxy)-3,3-dimethylbutan-2-ol in 200 ml of dry dimethyl sulfoxide, and the mixture was stirred at 120° C. until the starting compound was no longer detectable by high-pressure liquid chromatography (HPLC). Thereafter, the mixture was cooled, water was added, the mixture was extracted twice with the same volume of ethyl acetate, the extracts were dried and the solvent was distilled off under reduced pressure.

Provenance & Evidence