HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 13533194, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 20267561 | HCID 20267561 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 13533194 | HCID 13533194 | — |
Reaction Steps
1.2 g of the compound obtained in Example 24 was dissolved in 10 ml of a 6N solution of hydrogen chloride in dioxane, and the resulting solution was stirred at room temperature for 2 hours. Then, ether was added thereto so as to cause crystallization. The precipitated crystals were separated by filtration and washed with ether to obtain 1.0 g of the desired compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539150 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-80d898f6afdb46ef881ed22ba9f26c76 |
| Source note | uspto-grants-1985_09 |