HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(7-Carboxyhept-6-enyl)-2-(1-imidazolyl)-3-methylindole → 1-(7-Carboxyheptyl)-2-(1-imidazolyl)-3-methylindole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(7-Carboxyhept-6-enyl)-2-(1-imidazolyl)-3-methylindole | HCID 53952730 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-(7-Carboxyheptyl)-2-(1-imidazolyl)-3-methylindole | HCID 13491438 | — |
Reaction Steps
1-(7-Carboxyhept-6-enyl)-2-(1-imidazolyl)-3-methylindole (20 mg) is dissolved in 1 ml of absolute ethanol with a catalytic amount of 10% palladium on charcoal and hydrogenated at 1 atmosphere pressure. After one mole of hydrogen is consumed the catalyst is removed by filtration and washed with a few milliliters of ethanol. The combined filtrates are concentrated to yield the 1-(7-carboxyheptyl)-3-methyl-2-(1-imidazolyl)indole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04539410 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-90972f49d616455ca289ec3e4aa1686f |
| Source note | uspto-grants-1985_09 |