HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → HCID 57152418, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | Ammonium Chloride | HCID 25517 | — |
| Reactant | HCID 20266877 | HCID 20266877 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57152418 | HCID 57152418 | — |
Reaction Steps
The crude 3-bromopropylphosphoramidic dichloride was added to a solution of 10 g of ammonia in 125 mL CH2Cl2 at -30° C. The resulting mixture of product and NH4Cl weighed 19.4 g. Extraction with CH2Cl2 gave a material which slowly discolored over several days, mp. 60°-65° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04540428 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-fad859f556494300ba1a37e26faa7d65 |
| Source note | uspto-grants-1985_09 |