反应详情

To a solution of 1.63 g (5 mmol) of the product of Example 26 in 10 ml of acetone, 1.41 g (10 mmol) methyl iodide were added and the mixture was refluxed overnight while stirring. The acetone layer was separated by decantation and the yellowish, oily residue was crystallized from methanol/ether.

1. temperaturethe mixture was refluxed overnight
2. customThe acetone layer was separated by decantation
3. customthe yellowish, oily residue was crystallized from methanol/ether