HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide → HCID 70475162, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide | HCID 6228 | — |
| Reactant | Sodium Cyanide | HCID 8929 | — |
| Reactant | 2-(Chloromethyl)-1-methylnaphthalene | HCID 19995184 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 70475162 | HCID 70475162 | — |
Reaction Steps
A mixture of 6.0 g of 2-chloromethyl-1-methylnaphthalene, 3.0 g of sodium cyanide and 75 ml of dimethylformamide was stirred for two hours at room temperature. Water (150 ml) was then added and stirring continued for one hour longer. The solid which had separated was collected by filtration and dried to give 5.0 g of 1-methylnaphthaleneacetonitrile as a pale tan solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04540705 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-c35e6ac8fab04b8bb727ac61ee55cbeb |
| Source note | uspto-grants-1985_09 |