2-Ethylhexyl acrylate → HCID 54203006, Verbindung

HRID 1719574Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 1719574
[C:1]([C:5]1[CH:10]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:8]=[C:7]([SH:15])[C:6]=1[OH:16])([CH3:4])([CH3:3])[CH3:2].[C:17]([O:21][CH2:22][CH:23]([CH2:28][CH3:29])[CH2:24][CH2:25][CH2:26][CH3:27])(=[O:20])[CH:18]=[CH2:19].C(N(CC)CC)C>C1(C)C=CC=CC=1>[CH2:28]([CH:23]([CH2:24][CH2:25][CH2:26][CH3:27])[CH2:22][O:21][C:17](=[O:20])[CH2:18][CH2:19][S:15][C:7]1[CH:8]=[C:9]([C:11]([CH3:14])([CH3:13])[CH3:12])[CH:10]=[C:5]([C:1]([CH3:4])([CH3:2])[CH3:3])[C:6]=1[OH:16])[CH3:29]

Komponenten

5

Edukt 3

HCID 76362-Ethylhexyl acrylateHCID 8471TriethylamineHCID 3041162Phenol, 2,2-bis(1,1-dimethylethyl)-6-mercapto-

Produkt 1

HCID 54203006HCID 54203006, VerbindungAusbeute 35 %

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 1140TolueneLösungsmittel

Versuchsvorschrift

The procedure of Example 1 was repeated using 20.0 grams of 2,4-di-tert-butyl-6-mercaptophenol, 15.5 grams of 2-ethylhexyl acrylate, 0.25 ml of triethylamine and 150 mls of toluene. The residue was purified by chromatography on silica gel using toluene/heptane eluent to give 12.4 g (35% yield) of a colorless oil.

Aufarbeitung

  1. customThe residue was purified by chromatography on silica gel

Quellen und Nachweise

ORD-Eintrag
ord-49c3145582fc4d3f9b5cc9b59cdae779
Quelldatensatz
uspto-grants-1985_09
Patentnummer
US04540732

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