HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Ethylhexyl acrylate → HCID 54203006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Ethylhexyl acrylate | HCID 7636 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Phenol, 2,2-bis(1,1-dimethylethyl)-6-mercapto- | HCID 3041162 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 54203006 | HCID 54203006 | 35% |
Reaction Steps
The procedure of Example 1 was repeated using 20.0 grams of 2,4-di-tert-butyl-6-mercaptophenol, 15.5 grams of 2-ethylhexyl acrylate, 0.25 ml of triethylamine and 150 mls of toluene. The residue was purified by chromatography on silica gel using toluene/heptane eluent to give 12.4 g (35% yield) of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04540732 |
| Source dataset | uspto-grants-1985_09 |
| ORD ID | ord-49c3145582fc4d3f9b5cc9b59cdae779 |
| Source note | uspto-grants-1985_09 |