HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Octanol → Dicaprylyl Ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Octanol | HCID 957 | — |
| Reactant | Sulfosuccinic acid monosodium salt | HCID 21220 | — |
| Solvent | Water | HCID 962 | — |
| Product | Dicaprylyl Ether | HCID 12399 | — |
Reaction Steps
206 kg (1581.8 moles) of n-octanol were heated to 190°-210° C. together with 2.94 kg of sulfosuccinic acid (70% by weight). The water of reaction formed was distilled off. After 7 hours, 10.3 g of 50% by weight sodium hydroxide were added to the cooled reaction mixture for neutralization, after which the crude product was washed until neutral and then distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05503760 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-e296b566e6b848bf9c01de3be92734cb |
| Source note | uspto-grants-1996_04 |