Benzyl Bromide → HCID 22419805, compound

Participants

Reaction Steps

To a solution of 2,0 g (~8,4 mmol) 7-chloro-8-cyano-1-hydroxyquinoxaline-2,3(1H,4H)-dione in a mixture of 150 ml ethanol and 175 ml 0,1M phosphate buffer pH 7.4 was added 3.0 g (~17,4 mmol) of benzylbromide. Stirring was continued for 20 h at 24° C. The precipitate was filtered off to give the title compound (2.7 g; 98%), m.p. 227°-229° C.

Provenance & Evidence