HuagongsheHuagongshe Chemistry Print Report · For research reference only
Nitromethane → HCID 53750430, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Nitromethane | HCID 6375 | — |
| Reactant | Ammonium Acetate | HCID 517165 | — |
| Reactant | HCID 22419951 | HCID 22419951 | — |
| Product | HCID 53750430 | HCID 53750430 | — |
Reaction Steps
The aidehyde 5-phenethyl-3-formylindole (0.15 g, 0.6 mmol), nitromethane (0.9 ml) and ammonium acetate (0.05 g, 0.7 mmol) were heated gently under reflux for 0.5 h. On cooling, crystals slowly separated. Crystallization from methanol gave of 5-(2-phenylethyl)-3-(2-nitroethenyl)indole as crystals.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504101 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-0af00cb5f4664397a49ecca55153c728 |
| Source note | uspto-grants-1996_04 |