Trifluoroacetic acid → HCID 18655293, compound

HRID 1720087Notes

Reaction equation

HRID 1720087 reaction equation
[F:1][C:2]([F:7])([F:6])[C:3]([OH:5])=[O:4].[CH2:8]([NH:15][C:16](=[O:27])[C@H:17]([CH2:24]CC)[NH:18][CH2:19][C@@H:20]([NH2:23])[CH2:21][SH:22])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.C(C(O)=O)(F)(F)F>O>[F:1][C:2]([F:7])([F:6])[C:3]([OH:5])=[O:4].[CH2:8]([NH:15][C:16](=[O:27])[C@H:17]([CH3:24])[NH:18][CH2:19][C@@H:20]([NH2:23])[CH2:21][SH:22])[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

Participants

4

Reactant 2

HCID 6422Trifluoroacetic acidHCID 18655306HCID 18655306, compound

Product 1

HCID 18655293HCID 18655293, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

N-(3-mercapto-2(R)-aminopropyl)-L-norvaline-benzyl amide trifluoroacetate salt, mp 60°-67° C. Anal. Calcd for C16H27N3OS. 2 CF3CO2H. 0.84 H2O: C, 42.37; H, 5.37; N, 7.80. Found: C, 42.42; H, 5.21; N, 7.45.

Sources & evidence

ORD record
ord-636c141d2de24a5b956af8cffc124a86
Source dataset
uspto-grants-1996_04
Patent number
US05504115

Reaction notes

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