HuagongsheHuagongshe Chemistry Print Report · For research reference only
Succinic anhydride → 4-Oxo-4-(4-pentylphenyl)butanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Succinic anhydride | HCID 7922 | — |
| Reactant | Pentylbenzene | HCID 10864 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Product | 4-Oxo-4-(4-pentylphenyl)butanoic acid | HCID 2063246 | — |
Reaction Steps
Succinic anhydride (8.6 g; 0.1 mole) is reacted with pentylbenzene (100 ml) and aluminum chloride (29 g; 0.22 mole) and the product isolated by the manner described in Example 3. Recrystallization from aqueous ethanol gives 3-(4-n-pentylbenzoyl)propanoic acid (17 g) as colorless crystals, m.p. 98°-100° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504244 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-b648181de95f4710a769cec70c4b1e09 |
| Source note | uspto-grants-1996_04 |