HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54488363, compound → HCID 54164563, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54488363 | HCID 54488363 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54164563 | HCID 54164563 | — |
Reaction Steps
2.4 g of N-(2-ethoxycarbonyl-3-phenylpropyl)-L-valine benzyl ester is dissolved in 50 mL of ethanol, to which is added 500 mg of 10% Pd-C, and the mixture is hydrogenated at 50 psi for 3 h. The resulting mixture is filtered and the solvent removed with a rotoevaporator to afford N-(2-ethoxycarbonyl-3-phenylpropyl)-L-valine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05504070 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-3ebb907a339047cbbfe4f006063c7f82 |
| Source note | uspto-grants-1996_04 |