HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131719370, compound → HCID 131719369, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131719370 | HCID 131719370 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 131719369 | HCID 131719369 | — |
Reaction Steps
Crude BOC-Ala-PA-DOTA from above was dissolved in trifluoroacetic acid (3.5 mL) and immediately evaporated to dryness under a stream of dry nitrogen. The solid residue was triturated twice with ether (15 mL) and twice with THF (15 mL) to give L-Ala-PA-DOTA (0.066 g: MF (FAB) m/e 617 (positive ion M+Na).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05505931 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-7b805072850a4c0682bdef891b7b797f |
| Source note | uspto-grants-1996_04 |