HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 53887707, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Propanehydrazonoyl chloride, N-(4-chlorophenyl)-2-oxo- | HCID 2771515 | — |
| Solvent | Triethylamine | HCID 8471 | — |
| Product | HCID 53887707 | HCID 53887707 | 96% |
Reaction Steps
The reaction of 4.47 g of 1-chloro-1-[(4-chlorophenyl) hydrazono]-2-propanone with 3.43 g of 4-chlorothiophenol and 3.36 ml of triethylamine as Example 11 yielded 6.3 g of 1-[(4-chlorophenyl)thio]-1-[(4-chlorophenyl)hydrazono]-2-propanone, mp 164°-167° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-01aed47fbe724b3fa14b01bbbb1871a1 |
| Source note | uspto-grants-1996_04 |