HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 54023508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | HCID 3830189 | HCID 3830189 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54023508 | HCID 54023508 | 87.6% |
Reaction Steps
The reaction of 2.88 g (0.0136 mol)of 1-chloro-1-[(3-methylphenyl)hydrazono]-2-propanone with 2.10 g of 4-chlorothiophenol and 2.04 ml of triethyl amine in 35 ml of ethanol as Example 11 yielded 3.8 g of 1-[(4-chlorophenyl)thio]-1-[(3-methylphenyl)hydrazono]-2-propanone, mp 112°-114° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-18bc915bd36948c8b5fb85910ef43d4b |
| Source note | uspto-grants-1996_04 |