HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Chlorothiophenol → HCID 53834495, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Chlorothiophenol | HCID 7815 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Propanehydrazonoyl chloride, N-(4-methylphenyl)-2-oxo- | HCID 2771523 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53834495 | HCID 53834495 | — |
Reaction Steps
The reaction of 4.07(0.0193 mol) g of 1-chloro-1-[(4-methylphenyl-)hydrazono]-2-propanone, 3.43 g of 4-chlorothiophenol and 3.36 ml of triethylamine in 40 ml of ethanol as in Example 11 yielded 5.55 g of 1-[(4-chlorophenyl)thio]-1-[(4-methylphenyl)hydrazono]-2-propanone, mp 133°-135.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-8a29208b87914a71b670467bb7ab1dda |
| Source note | uspto-grants-1996_04 |