p-Chlorothiophenol → HCID 54054985, compound

HRID 1720246Notes

Reaction equation

HRID 1720246 reaction equation
Cl[C:2](=[N:6][NH:7][C:8]1[CH:13]=[CH:12][C:11]([Br:14])=[CH:10][CH:9]=1)[C:3](=[O:5])[CH3:4].[Cl:15][C:16]1[CH:21]=[CH:20][C:19]([SH:22])=[CH:18][CH:17]=1.C(N(CC)CC)C>C(O)C>[Cl:15][C:16]1[CH:21]=[CH:20][C:19]([S:22][C:2](=[N:6][NH:7][C:8]2[CH:13]=[CH:12][C:11]([Br:14])=[CH:10][CH:9]=2)[C:3](=[O:5])[CH3:4])=[CH:18][CH:17]=1

Participants

5

Reactant 3

HCID 7815p-ChlorothiophenolHCID 8471TriethylamineHCID 2771519HCID 2771519, compound

Product 1

HCID 54054985HCID 54054985, compound

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

1-chloro-1-[(4-bromophenyl)hydrazono]-2-propanone is reacted with 4-chlorothiophenol and triethyl amine in ethanol as Example 11 to yield 1-[(4-chlorophenyl)thio]-1-[(4-bromophenyl)hydrazono]-2-propanone.

Sources & evidence

ORD record
ord-a2b9d2464dc345b596404056dad39a7f
Source dataset
uspto-grants-1996_04
Patent number
US05506228

Reaction notes

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