HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 53927081, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Propanehydrazonoyl chloride, N-(4-methoxyphenyl)-2-oxo- | HCID 2844936 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 53927081 | HCID 53927081 | 84.7% |
Reaction Steps
The reaction of 392 mg of 1-chloro-1-[(4-methoxyphenyl) hydrazono]-2-propanone, 220 mg of thiophenol and 280 ul of triethylamine in 6 ml of ethanol as in Example 11 yielded 440 mg of 1-[(phenyl)thio]-1-[(4-methoxyphenyl)hydrazono]-2-propanone, mp 120°-123° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506228 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-5b82f80352b8494abd11902c46fa4986 |
| Source note | uspto-grants-1996_04 |