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HRID1720250

反应详情

EQUATION

反应方程式

HRID 1720250 的结构方程式

REACTANTS

反应物

4
结构：CC(C)=O
HCID180

Acetone

C3H6O

结构：CC(=O)[O-].[NH4+]
HCID517165

Ammonium acetate

C2H7NO2

结构：Cc1c(Sc2ccc(Cl)cc2)nn(-c2ccc(Cl)cc2)c(=O)c1C#N
HCID15293922

未命名化合物

结构：CCOC(=O)C(C#N)C1(C#N)CCCC1
HCID16226777

Ethyl cyano(1-cyanocyclopentyl)acetate

C11H14N2O2

PRODUCTS

生成物

1
结构：Cc1c(Sc2ccc(Cl)cc2)nn(-c2ccccc2)c(=O)c1C#N
HCID22417686

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

The reaction of 1.8 g (5.9 mmol) of 1-[(4-chlorophenyl)thio]-1-[phenyl)hydmzono]-2-propanone, 1.5 ml of ethylcyano acetate and 750 mg of ammonium acetate as in Example 22, yielded1.29 g of 6-[(4-chlorophenyl)thio]- 2,3-dihydro-2-(4-chlorophenyl)5-methyl-3-oxo-4-pyridazinecarbonitrile, mp 180°-182° C. (EtOH).