Dodecylamine → HCID 22417912, compound

HRID 1720282Notes

Reaction equation

[Cl:1][C:2]1[C:11]2[C:6](=[C:7]([OH:12])[CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][CH:3]=1.[CH2:13]([NH2:25])[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]>>[ClH:1].[CH2:13]([NH:25][C:2]1[C:11]2[C:6](=[C:7]([OH:12])[CH:8]=[CH:9][CH:10]=2)[N:5]=[CH:4][CH:3]=1)[CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH2:22][CH2:23][CH3:24]

Participants

Reactant 2

HCID 13583Dodecylamine

HCID 3841644-chloroquinolin-8-ol

Product 1

HCID 22417912HCID 22417912, compound

Procedure

In a manner similar to that described in Example 49, Part B, 4-chloroquinolin-8-ol and n-dodecylamine were transformed into the title compound: m.p. 189°-190° C.; m/e 328 (molecular ion); NMR spectum consistent with assigned structure.

Sources & evidence

ORD record: ord-cf96f6dbc8a9440784c683f315e42acd
Source dataset: uspto-grants-1996_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05506235

Reaction notes

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