Methylamine → HCID 10979878, compound

HRID 1720373Notes

Reaction equation

HRID 1720373 reaction equation
[CH3:1][O:2]/[N:3]=[C:4](\[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][O:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[CH3:23])/[C:5](OC)=[O:6].[CH3:24][NH2:25]>>[CH3:24][NH:25][C:5](=[O:6])/[C:4](=[N:3]/[O:2][CH3:1])/[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[CH2:15][O:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=1[CH3:23]

Participants

3

Reactant 2

HCID 6329MethylamineHCID 6112114Kresoxim-methyl

Product 1

HCID 10979878HCID 10979878, compound

Conditions

Temperature
40 °C

Procedure

250 g of methyl E-2-methoxyimino-2-[(2-methylphenoxymethyl)phenyl]acetate are suspended in 1 l of 40% strength aqueous methylamine solution and heated at 40° C. for 4 h. After cooling to room temperature (20° C.), the solid is filtered off with suction, washed several times with water and dried at 50° C. 229.8 g of the title compound are obtained as colorless crystals.

Workup

  1. temperatureAfter cooling to room temperature (20° C.)
  2. filtrationthe solid is filtered off with suction
  3. washwashed several times with water
  4. customdried at 50° C

Sources & evidence

ORD record
ord-35713ac333164e7f9a296aa1ce6ccd66
Source dataset
uspto-grants-1996_04
Patent number
US05506254

Reaction notes

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