HRID1720448

反应详情

EQUATION

反应方程式

HRID 1720448 的结构方程式

PROCEDURE

实验过程

To a mixture of concentrated NH4OH (100 mL) and ice was added 2-thiopheneacetyl chloride (13.0 g, 80.9 mmol). The desired compound crystallized from the reaction mixture. Recrystallization from hot water gave 2-thiopheneacetamide (8.08 g, 64% yield) as white crystals. mp 146°-147° C.

WORKUP

后处理

  1. customThe desired compound crystallized from the reaction mixture
  2. customRecrystallization from hot water