HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → HCID 22418605, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | HCID 53712566 | HCID 53712566 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 22418605 | HCID 22418605 | 99% |
Reaction Steps
A solution of 7-octadecylcarbamoyloxy-6-palmitoyloxy-4-thiaheptanoic acid t-butyl ester as obtained in Reference Example 8 (3.425 g) in trifiuoroacetic acid (5 ml)-dichloromethane (3 ml) was stirred at room temperature for 1 hour, followed by solvent concentration under reduced pressure, to yield the title compound (3.14 g, yield 99%) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506267 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-42ed6d19b0974ef693d3e552f7f107e1 |
| Source note | uspto-grants-1996_04 |