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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1720790Generated: November 2, 2026

Dichloromethane → HCID 22418605, compound

https://huagongshe.com/reaction/1720790

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDichloromethaneHCID 6344—
ReactantHCID 53712566HCID 53712566—
SolventTrifluoroacetic acidHCID 6422—
ProductHCID 22418605HCID 2241860599%

Reaction Steps

A solution of 7-octadecylcarbamoyloxy-6-palmitoyloxy-4-thiaheptanoic acid t-butyl ester as obtained in Reference Example 8 (3.425 g) in trifiuoroacetic acid (5 ml)-dichloromethane (3 ml) was stirred at room temperature for 1 hour, followed by solvent concentration under reduced pressure, to yield the title compound (3.14 g, yield 99%) as a colorless solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05506267
Source datasetuspto-grants-1996_04
ORD IDord-42ed6d19b0974ef693d3e552f7f107e1
Source noteuspto-grants-1996_04