HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dichloromethane → 6,7-Bis(octadecylcarbamoyloxy)-4-thiaheptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | 6,7-Bis(octadecylcarbamoyloxy)-4-thiaheptanoic acid t-butyl ester | HCID 53926087 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | 6,7-Bis(octadecylcarbamoyloxy)-4-thiaheptanoic acid | HCID 22418623 | 99% |
Reaction Steps
A solution of 6,7-bis(octadecylcarbamoyloxy)-4-thiaheptanoic acid t-butyl ester as obtained in Reference Example 7 (1010 mg) in trifiuoroacetic acid (3 ml)-dichloromethane (0.5 ml) was stirred at room temperature for 1 hour, followed by solvent concentration under reduced pressure, to yield the title compound (938 mg, yield 99%) as a colorless solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506267 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-09bb160174b84a9c93262a57769a540c |
| Source note | uspto-grants-1996_04 |