HRID1720791
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 6,7-bis(octadecylcarbamoyloxy)-4-thiaheptanoic acid t-butyl ester as obtained in Reference Example 7 (1010 mg) in trifiuoroacetic acid (3 ml)-dichloromethane (0.5 ml) was stirred at room temperature for 1 hour, followed by solvent concentration under reduced pressure, to yield the title compound (938 mg, yield 99%) as a colorless solid.
WORKUP
后处理
- concentrationfollowed by solvent concentration under reduced pressure