HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → 6,7-Bis(12-phenyldodecanoyloxy)-4-thiaheptanoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | 6,7-Bis(12-phenyldodecanoyloxy)-4-thiaheptanoic acid t-butyl ester | HCID 54116109 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 6,7-Bis(12-phenyldodecanoyloxy)-4-thiaheptanoic acid | HCID 22418617 | 99% |
Reaction Steps
A solution of 6,7-bis(12-phenyldodecanoyloxy)-4-thiaheptanoic acid t-butyl ester as obtained in Reference Example 33 (1.22 g) in dichloromethane (2 ml)-trifluoroacetic acid (6 ml) was stirred at room temperature for 2 hours, after which the solvent was distilled off under reduced pressure, to yield the title compound (1.12 g, yield 99%) as a colorless oily substance.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506267 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-9ab0196d75684eb892986ef6a42fd4a2 |
| Source note | uspto-grants-1996_04 |