HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → (6,7-Bis(palmi toyloxy)-4-thiaheptanoyl)glycylglycylglycine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | (6,7-Bis(palmitoyloxy)-4-thiaheptanoyl)glycylglycylglycine t-butyl ester | HCID 22418631 | — |
| Product | (6,7-Bis(palmi toyloxy)-4-thiaheptanoyl)glycylglycylglycine | HCID 22418620 | 86% |
Reaction Steps
(6,7-bis(palmitoyloxy)-4-thiaheptanoyl)glycylglycylglycine t-butyl ester as obtained in Example 5 (110 mg) was mixed with trifiuoroacetic acid (5 ml), followed by stirring at room temperature for 1 hour. The mixture was concentrated to yield the title compound (81 mg, yield 86%) as a colorless crystal.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05506267 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-96b46bfa02ea424c9898eec59b97bcac |
| Source note | uspto-grants-1996_04 |