HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 22416633, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | N-methylpropyn-2-ylamine | HCID 96160 | — |
| Reactant | Decane, 2-bromo- | HCID 98297 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22416633 | HCID 22416633 | 100% |
Reaction Steps
2-Bromodecane (8.84 g, 40 mmoles) and N-methylpropargylamine (5.52 g, 80 mmoles) were heated in absolute ethanol (50 mL) for 72 h. to give, after treatment with 40 mmoles of ethanolic hydrochloric acid, the title compound in a yield of 100% (75% after recrystallization from methanol-ether), m.p.=130°-131° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05508311 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-2a448ee7b8314656a5b6c8064dcd5188 |
| Source note | uspto-grants-1996_04 |