Hydrochloric Acid → HCID 22416633, compound

HRID 1720972Notes

Reaction equation

HRID 1720972 reaction equation
Br[CH:2]([CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11])[CH3:3].[CH3:12][NH:13][CH2:14][C:15]#[CH:16].[ClH:17]>C(O)C>[ClH:17].[CH3:3][CH:2]([N:13]([CH2:14][C:15]#[CH:16])[CH3:12])[CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH3:11]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 96160N-methylpropyn-2-ylamineHCID 982972-Bromodecane

Product 1

HCID 22416633HCID 22416633, compoundYield 100%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

2-Bromodecane (8.84 g, 40 mmoles) and N-methylpropargylamine (5.52 g, 80 mmoles) were heated in absolute ethanol (50 mL) for 72 h. to give, after treatment with 40 mmoles of ethanolic hydrochloric acid, the title compound in a yield of 100% (75% after recrystallization from methanol-ether), m.p.=130°-131° C.

Workup

  1. customto give

Sources & evidence

ORD record
ord-2a448ee7b8314656a5b6c8064dcd5188
Source dataset
uspto-grants-1996_04
Patent number
US05508311

Reaction notes

Loading…