HRID1721175

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID138566

2,2-Diethylbutanedioic acid

C8H14O4

HCID253877

Potassium bromide

BrK

结构：Nc1cccc(OCc2ccc3ccc(OCc4ccccc4)cc3n2)c1

HCID22416907

未命名化合物

PRODUCTS

生成物

结构：CCC(CC)(CC(=O)Nc1cccc(OCc2ccc3ccc(OCc4ccccc4)cc3n2)c1)C(=O)O

HCID22416871

未命名化合物

PROCEDURE

实验过程

Analogously to Example 3, the title compound is prepared starting from 3-(7-benzyloxy-2-quinolinylmethoxy)aniline and 2,2-diethylsuccinic acid. Slightly yellowish crystals of m.p. 89°-95° are obtained; IR (KBr): 3325, 2966, 1689, 1599, 1545, 1512, 1492, 1436, 1380, 1208, 1157, 1024, 842, 775, 695 cm-1.

WORKUP

后处理

customSlightly yellowish crystals of m.p. 89°-95° are obtained

来源与证据

来源类型: Open Reaction Database
ORD 记录: ord-2f1ed7585b724bcaabee9866c4f12fc6
来源数据集: uspto-grants-1996_04
DOI: 10.6084/m9.figshare.5104873.v1
专利: US05508408
来源说明: uspto-grants-1996_04

反应 SMILES

[CH2:1]([O:8][C:9]1[CH:18]=[C:17]2[C:12]([CH:13]=[CH:14][C:15]([CH2:19][O:20][C:21]3[CH:22]=[C:23]([CH:25]=[CH:26][CH:27]=3)[NH2:24])=[N:16]2)=[CH:11][CH:10]=1)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:28]([C:30]([CH2:38][CH3:39])([CH2:34][C:35](O)=[O:36])[C:31]([OH:33])=[O:32])[CH3:29].[K+].[Br-]>>[CH2:1]([O:8][C:9]1[CH:18]=[C:17]2[C:12]([CH:13]=[CH:14][C:15]([CH2:19][O:20][C:21]3[CH:22]=[C:23]([NH:24][C:35](=[O:36])[CH2:34][C:30]([CH2:38][CH3:39])([CH2:28][CH3:29])[C:31]([OH:33])=[O:32])[CH:25]=[CH:26][CH:27]=3)=[N:16]2)=[CH:11][CH:10]=1)[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1