Hydrochloric Acid → HCID 22414129, compound

HRID 1721402Notes

Reaction equation

HRID 1721402 reaction equation
Cl.[CH2:2]([N:20](C)[C:21]1[CH:26]=[CH:25][C:24]([N+:27]([O-])=O)=[CH:23][CH:22]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19].[CH2:31](O)C>>[CH2:2]([NH:20][C:21]1[CH:22]=[CH:23][C:24]([NH:27][CH3:31])=[CH:25][CH:26]=1)[CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH3:19]

Participants

4

Reactant 3

HCID 313Hydrochloric AcidHCID 702EthanolHCID 53912005HCID 53912005, compound

Product 1

HCID 22414129HCID 22414129, compound

Procedure

100 ml 2N hydrochloric acid is added to a solution of which 60.6 g (0.15 mol) N, N-octadecylmethyl- p-nitroaniline is dissolved into 500 ml ethyl alcohol. 52.5 g (0.13 mol) N, N-octadecylmethyl-p-phenylenediamine is obtained after adding 48.8 g (0.75 mol) zinc dust to the solution and heat and reflux it for one hour.

Sources & evidence

ORD record
ord-d33a28d9fb3548ef82b43b10548bae6a
Source dataset
uspto-grants-1996_04
Patent number
US05510224

Reaction notes

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