Benzoic Acid → HCID 569544, compound

HRID 1721440Notes

Reaction equation

HRID 1721440 reaction equation
C(OC(=O)C)(=O)C.[C:8]([OH:16])(=O)[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1.[C:17]1(=[O:24])[NH:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18]1>C(O)(=O)C>[C:8]([CH:18]1[CH2:19][CH2:20][CH2:21][CH2:22][NH:23][C:17]1=[O:24])(=[O:16])[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

Participants

5

Reactant 3

HCID 243Benzoic AcidHCID 7768CaprolactamHCID 7918Acetic Anhydride

Product 1

HCID 569544HCID 569544, compound

Reagents, catalysts & solvents 1

HCID 176Acetic AcidSolvent

Procedure

heating acetic anhydride, benzoic acid, and caprolactam at a temperature of about 130° to about 170° C. to form volatile acetic acid and benzoyl caprolactam;

Sources & evidence

ORD record
ord-353b86007dc749c7a12df123b1d18c76
Source dataset
uspto-grants-1996_04
Patent number
US05510477

Reaction notes

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