HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-3-(4-benzyloxyphenyl)pyridazine → 3-(4-Benzyloxyphenyl)-6-(6-octyloxypyridin-3-yl)pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-3-(4-benzyloxyphenyl)pyridazine | HCID 22412630 | — |
| Reactant | 2-Octyloxy-5-pyridineboronic acid | HCID 22412798 | — |
| Product | 3-(4-Benzyloxyphenyl)-6-(6-octyloxypyridin-3-yl)pyridazine | HCID 22412938 | 69.3% |
Reaction Steps
In accordance with scheme D, 14 g (47.2 mmol) of 6-chloro-3-(4-benzyloxyphenyl)pyridazine are reacted analogously to Example 4a with 11.8 g (47.2 mmol) of 2-octyloxypyridine-5-boronic acid to give 15.3 g of 3-(4-benzyloxyphenyl)-6-(6-octyloxypyridin-3-yl)pyridazine.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05512207 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-1db1615caf5e4ca49c7eeaddec9730db |
| Source note | uspto-grants-1996_04 |