HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl iodide → HCID 178504025, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 10709059 | HCID 10709059 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 178504025 | HCID 178504025 | 84.3% |
Reaction Steps
A suspension of 4-(5-acetylaminomethylfuran-2-yl)-2-thioureidothiazole (12.6 g) and methyl iodide (7.2 g) in methanol (200 ml) was refluxed for 5.5 hours. The solvent was removed under reduced pressure. The residue was washed with ethyl acetate to afford 4-(5-acetylaminomethylfuran-2-yl)-2-(2-methylisothioureido)thiazole hydriodide (15.7 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05512588 |
| Source dataset | uspto-grants-1996_04 |
| ORD ID | ord-a23747c3f8d44b70808a00ae50cf0334 |
| Source note | uspto-grants-1996_04 |