HCID 19860393, compound → HCID 19860376, compound

Participants

Reaction Steps

A solution of 2-amino-N-(1,1-dimethylethyl)-4-[(3-methylphenyl)amino]-5-pyrimidinesulfonamide (0.90 gm, 0.0027 mol) in trifluoroacetic acid (10 mL) was heated to reflux for 1 hour. After cooling, the solvent was evaporated in vacuo and the resulting solid triturated with ether to give 0.50 g, 67% of product, m.p. 213°-215° C., as a colorless solid.

Provenance & Evidence