HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chlorobenzaldehyde → HCID 20030102, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chlorobenzaldehyde | HCID 6996 | — |
| Reactant | 6-Amino-1,3-dimethyluracil | HCID 81152 | — |
| Reactant | HCID 20070366 | HCID 20070366 | — |
| Product | HCID 20030102 | HCID 20030102 | 5.2% |
Reaction Steps
The title compound (150 mg) was prepared from 2-chlorobenzaldehyde (747 mg), 6-amino-1,3-dimethyl-2,4-dioxopyrimidine (824 mg) and methyl 4-[2-(2,4,5-trimethylimidazol-1-yl)propoxyl]3-oxobutanoate (1.5 g) by the method of Example 1. M.p. 180°-182° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853392 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-ee9924a21ea840498ce173c271e6a3c2 |
| Source note | uspto-grants-1989_08 |