HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → Ethyl-2-(2-propylimidazol-1-yl)propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Ethyl 2-bromopropionate | HCID 79040 | — |
| Reactant | 2-Propylimidazole | HCID 162617 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | Ethyl-2-(2-propylimidazol-1-yl)propanoate | HCID 20070368 | — |
Reaction Steps
2-Propylimidazole (5.5 g), ethyl 2-bromopropionate (9.95 g) and potassium carbonate (12.4 g) were stirred in refluxing acetonitrile (100 ml) for 72 hours. The suspension was allowed to cool, filtered and the solvent removed under reduced pressure, yielding the title compound as an off-white foam, 9.2 g [88%].
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853392 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-2bd3e86144384b45b2db53708bb5d401 |
| Source note | uspto-grants-1989_08 |