HRID1721885

反应详情

EQUATION

反应方程式

HRID 1721885 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

2-Propylimidazole (5.5 g), ethyl 2-bromopropionate (9.95 g) and potassium carbonate (12.4 g) were stirred in refluxing acetonitrile (100 ml) for 72 hours. The suspension was allowed to cool, filtered and the solvent removed under reduced pressure, yielding the title compound as an off-white foam, 9.2 g [88%].

WORKUP

后处理

  1. temperatureto cool
  2. filtrationfiltered
  3. customthe solvent removed under reduced pressure