HuagongsheHuagongshe Chemistry Print Report · For research reference only
Glycidol → HCID 13798875, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Glycidol | HCID 11164 | — |
| Reactant | Ethoxyethylamine | HCID 66970 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | HCID 13798875 | HCID 13798875 | 69.2% |
Reaction Steps
A solution of glycidol (15 g, 0.2 mol) in isopropanol (50 ml) was added dropwise under N2 at 70° C. to a solution of 2-ethoxyethylamine (53 g, 0.6 mol) in isopropanol (125 ml). After 15 hours, the isopropanol was removed under reduced pressure (20 mm) and the residue distilled at 120°-5° C. at 0.4 mm to yield 22.6 g (69%) of 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04853383 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-639f0ec039274968a09b646d3ce8405e |
| Source note | uspto-grants-1989_08 |