HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 14673794, compound → HCID 14673796, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 14673794 | HCID 14673794 | — |
| Catalyst | Palladium hydroxide | HCID 9942167 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14673796 | HCID 14673796 | — |
Reaction Steps
The N-benzylated amine from Step 5 (2.7 mmol) was dissolved in 30 mL of ethanol and treated with 1 mass equivalent of palladium hydroxide on carbon. This mixture was placed under an atmosphere of hydrogen gas, initially at 50 psi (445 kPa) for 12 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04855316 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-8ac3f96fd44845e99e2151dc1ceb5f96 |
| Source note | uspto-grants-1989_08 |