Hydrofluoric Acid → HCID 15053054, compound

HRID 1722389Notes

Reaction equation

HRID 1722389 reaction equation
[CH:1]1([CH2:6][CH2:7][CH2:8][CH2:9][O:10][Si](C(C)(C)C)(C)C)[CH2:5][CH2:4][CH:3]=[CH:2]1.F>C(#N)C>[OH:10][CH2:9][CH2:8][CH2:7][CH2:6][CH:1]1[CH2:5][CH2:4][CH:3]=[CH:2]1

Participants

4

Reactant 2

HCID 14917Hydrofluoric AcidHCID 13924077HCID 13924077, compound

Product 1

HCID 15053054HCID 15053054, compound

Reagents, catalysts & solvents 1

HCID 6342AcetonitrileSolvent

Procedure

The procedure followed is the same as that described in Example 12 substituting 3-(5-[(1,1-dimethylethyl)dimethylsiloxy]but-1-yl)cyclopentene {[4-(2-cyclopenten-1-yl)butoxy](1,1-dimethylethyl)dimethylsilane} (100 g, 0.407 moles), 5% hydrofluoric acid (78 ml), acetonitrile (1500 ml). The crude product is kugelrohred under reduced pressure leaving a clear, colorless oil (51 g, 0.36 moles).

Sources & evidence

ORD record
ord-33344588811146afabed4bf47f0f6728
Source dataset
uspto-grants-1989_08
Patent number
US04855322

Reaction notes

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