Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 14213086 | HCID 14213086 | — |
| Solvent | Water | HCID 962 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 14213088 | HCID 14213088 | 93% |
Reaction Steps
A solution of the product from Example 115 (2 g, 5.99 mmol) in dioxane (10 ml) was treated with 0.26 g (6.5 mmol) of sodium hydroxide in 5 ml of water. After stirring for 16 h at 35° C., the reaction was worked up as described in Example 114 to give a 93% yield of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04857507 |
|---|
| Source dataset | uspto-grants-1989_08 |
|---|
| ORD ID | ord-a2a581098dcc4e3b8ffd34b8b4106c62 |
|---|
| Source note | uspto-grants-1989_08 |
|---|
