Hydrochloric Acid → HCID 15052635, compound
Reaction equation
C[O:2][C:3](=[O:20])[C@H:4]([CH2:11][C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=1)[NH:5][C:6]([N:8]([CH3:10])[CH3:9])=[O:7].Cl>>[CH3:10][N:8]([CH3:9])[C:6]([NH:5][C@H:4]([C:3]([OH:20])=[O:2])[CH2:11][C:12]1[CH:17]=[CH:16][C:15]([O:18][CH3:19])=[CH:14][CH:13]=1)=[O:7]Participants
3
Procedure
Prepared according to the procedure of Example 130 from the resultant compound of Example 131 with the modification that the product was isolated by pouring the reaction mixture into 2 M HCl and extracting with ethyl acetate which was dried over Na2SO4 and evaporated. EI-MS: M+ =266.
Workup
- customPrepared
- customwas isolated
- extractionextracting with ethyl acetate which
- dry with materialwas dried over Na2SO4
- customevaporated
Sources & evidence
- ORD record
- ord-f5532b9dee444144a824764d502d6f14
- Source dataset
- uspto-grants-1989_08
- Patent number
- US04857507
Reaction notes
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