HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 54369785, compound → HCID 53671948, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 54369785 | HCID 54369785 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53671948 | HCID 53671948 | 97% |
Reaction Steps
The resultant compound from Example 144 (200 mg, 0.523 mmol) and 10% Pd on carbon (200 mg) in methanol (10 ml) were stirred under a hydrogen atmosphere for 3 h. The reaction was filtered and evaporated to afford 148 mg (97%) of the desired product as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857507 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-ce20a648af714842926b2cae260cfeb3 |
| Source note | uspto-grants-1989_08 |