HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 178456761, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | Potassium Fluoride | HCID 522689 | — |
| Reactant | HCID 178522677 | HCID 178522677 | — |
| Solvent | Dimethyl Sulfoxide | HCID 679 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178456761 | HCID 178456761 | — |
Reaction Steps
A mixture of 20 g (0.097 mol) of 4-fluoro-N-1H-tetrazol-5-ylbenzamide, 12.8 ml (0.193 mol) of propargylamine, 5.6 g of anhydrous potassium fluoride, and 13 g of potassium carbonate, in 320 ml of dimethylsulfoxide is heated at 50°-70° C. for six to twenty hours. The reaction is poured into water and the precipitate is collected, washed with water, and dried in vacuo to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857530 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-4257f44f38554c3e9c8c4201b1edf2f5 |
| Source note | uspto-grants-1989_08 |