HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 14054697, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 1-Fluoro-2-nitrobenzene | HCID 73895 | — |
| Reactant | 3,5-Difluorobenzylamine | HCID 145211 | — |
| Product | HCID 14054697 | HCID 14054697 | 100.9% |
Reaction Steps
Reaction of 2-fluoronitrobenzene (3 g, 21 mmole), 3,5-difluorobenzylamine, (3 g, 21 mmole) and triethylamine (2.6 g, 26.2 mmole) substantially as described in 1C above produced 5.6 g (100%) of title compound as orange crystals: mp 104°-105°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04857540 |
| Source dataset | uspto-grants-1989_08 |
| ORD ID | ord-b4471335d24747e78a4b4a8098e1fce4 |
| Source note | uspto-grants-1989_08 |